TJIIRRS: Number 5E [New] of an Ongoing Series;

“Theorie und Praxis Va”,
Simple and Effective Atmospheric Pressure Nitrogen Lasers
Part 1

Abstract:

This page follows the development of a straightforward TEA nitrogen laser design that is based on the excellent work of Jarrod S. Kinsey, and is intended for DIY construction. I hope to follow it with a second page that will detail the development of a high-performance TEA design, also intended for DIYers. (By “high performance” I mean well over a megawatt, perhaps several megawatts.)

I should perhaps point out that a megawatt is much easier to achieve with a TEA nitrogen laser than with what Jarrod refers to as a “TERP” laser (Transversely Excited [at] Reduced Pressure); this is because the pulsewidth is 1 nsec or less, so the energy in a 1-MW pulse is slightly less than 1 mj. A reduced-pressure nitrogen laser of an ordinary sort, on the other hand, must put out 6-10 mj in order to reach 1 megawatt peak power, because it produces a much longer pulse.

Because the pulse from a TEA nitrogen laser is less than 1 nsec long FWHM (“Full Width at Half Maximum amplitude”), good design and implementation are crucial for high performance. The odd and interesting issue that informs this page is that it turns out to be remarkably straightforward to design and construct a room-pressure nitrogen laser if one is even slightly less concerned about optimization. These lasers are considerably easier and less complex than the 1974 Scientific American Amateur Scientist laser.

Either a small “TERP” or one of these TEA lasers can easily be powered by and electrostatic generator, as Jarrod has demonstrated and as you can see on his Website (link, above). In fact, I use a little Wimshurst machine to run most of the lasers on this page.

I should note once again that the designs shown here are based on Jarrod Kinsey’s, and that my understanding of the issues involved in their operation owes a huge debt both to him and to Milan Karakas, who taught himself to produce clean glow discharges in air at room pressure, and was kind enough to share his knowledge, experience, and insights. Milan also tweaked one of the photos shown below.



!! CAUTION !!

1. These lasers use high voltages, and capacitors that can store significant amounts of energy. A nitrogen laser puts out an invisible ultraviolet beam that can damage your eyes and skin. It is important to take adequate safety precautions and use appropriate safety equipment with any laser; but it is crucially important with lasers that involve high voltages and/or produce invisible beams!

2. When you fire a laser that stores substantial amounts of energy and discharges that energy in a very short time, you generate a sharp electromagnetic pulse. This pulse radiates out from the laser circuitry, and can damage equipment that is connected to the laser, or even close to it. I always put one or more large inductors “hot” line from the power supply, and also one in the ground line. (This and the following assume a regular electrical or electronic supply, rather than an electrostatic one. Electrostatic supplies do not need chokes.) If you are attempting to measure the output of your power supply with a voltage divider, put a smaller choke in each of the wires going to the meter, as close to it as possible. You probably also want to put a small capacitor directly across the meter input, as an additional “snubber”. (Again, if you are fortunate enough to have a pure electrostatic voltmeter, it is probably unnecessary to protect it, and putting a capacitor across its input may not be a good idea unless you are using a voltage divider, as the input impedance of a good ESVM is 1015 ohms.)



Image Note

If you click any of the small photos or images (except for the schematic diagram, which is already full size), you’ll get a bigger one. Most of them are 1280 px across (“.12c.” in the filename), or 1280 px high if they are in portrait orientation, (“.c12.” in the filename) though some portrait-mode images may be 1024 px high (“.c10.” in the filename). A filename preceded by a lowercase c is a picture I took with a Canon G3; one that is preceded by a lowercase s was taken with a Sony DSC-R1. If this is not specified in the filename or the text, any photo showing a discharge was taken with the Canon, and any other photo could be from either camera.

A Canon image probably also exists in 22c or c22 size if you want more pixels; a Sony original likewise probably also exists in 38c or c38 size. The exceptions are crops, which have a lowercase c after the file number, as for example “1848c.manthebarricades.8c.jpg”. I generally try to list the largest available size of a cropped image.

For those who bother to read things like filenames, I will note that I do not actually have photos from any of the 1848 revolutions. (Pyrogallol, the first really successful photographic developer, was not introduced until 1851.)



Initial Considerations and Design Issues

(20 March, 2007)

There are only a few viable methods for achieving a clean and sufficiently fast discharge in nitrogen at 1 atm. partial pressure, or in air. All of them involve significant levels of preionization; without this, it is essentially impossible to avoid sparking. The preionization can be present as a side-effect of the design or as a deliberately introduced feature, it can be inherent and automatic, or it can be externally timed and driven; but one way or the other, it must occur. (Externally controlled preionization is not particularly viable for TEA nitrogen lasers because the timing requirements are so tight. Fortunately, it turns out to be quite easy to have the laser preionize itself.)

Higher voltage is hard on dielectrics, but it provides compensating advantages; the amount of energy stored in a given capacitor increases with the square of the applied voltage, while the speed of the discharge (all other things being equal) decreases with the square root of the capacitance. Again, thinner dielectrics have higher capacitance per unit area, allowing the use of smaller plates; and they also have reduced inductance, which helps speed up the discharge.

It is likely that a cylindrical capacitor is the fastest physical configuration, btw; and in fact I have been told that a cylindrical water-cap that was resonantly charged to 120 kV by a 3-stage Marx bank was sufficient to operate a TEA nitrogen laser at well over 10 MW. That level of complexity is outside the scope of this page, though I do anticipate investigating cylindrical capacitors (and liquid dielectrics) in the followup project. I have already constructed a “TERP” nitrogen laser that uses a liquid dielectric in its peaker capacitor.

If you are having serious trouble achieving a clean discharge in air, it can be helpful to use nitrogen, or a mixture of nitrogen and helium in roughly equal proportions (though this will result in a longer pulse). Either of these, however, fails to guide you through the process of learning to produce a clean glow discharge in air, so you should think of it as a set of training wheels, rather than as your main approach. It is much better to learn to lase air first, and only then to make the transition to pure nitrogen.

Dielectric constant and dielectric strength are crucial issues. Water has dielectric constant of about 80, and impressive dielectric strength. It is, moreover, self-healing. Unfortunately, it must be extremely pure in order to work well, and because it is a liquid it tends to leak. For these reasons I am going to bypass it, at least in the early stages of the project. It may find some use when I get to cylindrical capacitors, or to a Charge-Transfer type of circuit, where the capacitor that drives the laser channel is charged only for a few dozen nsec..

I had anticipated switching the first laser for this page with an EG&G GP-20 spark gap, which is quite small and is rated only for voltages up to about 11 kV, but I couldn’t find it, so I used a GP-70 instead. The GP-70 is physically larger, and thus has more inductance (it takes the current-carrying path farther away from the baseplate), which can be a serious issue. In fact, I ended up going to a free-running open spark gap in order to get closer to Jarrod’s designs, as they are known to work and do not involve any expensive components. (There are more details about this below.)

The simplest TEA nitrogen lasers are built as LC-inversion circuits:

(I used a charging resistor instead of a charging inductor; but either, or a combination, can be made to work.) The small capacitor that appears just above the laser channel is one possible method for preionizing the channel. It was suggested by Milan Karakas, as a sliding or surface discharge: a piece of brass shim stock is connected to the anode side of the laser; it extends out on top of the top wall of the channel, which is a thin glass plate, and covers most (but not quite all) of the channel. This shim must be insulated from the cathode so it does not arc over the outside of the wall and thus short-circuit the discharge. In operation, as the voltage across the channel begins to increase, the voltage at the glass surface near the cathode rises very quickly because the brass shim is very close. This causes a surface-corona effect, which injects UV and ions into the channel, preionizing it. I have not built a channel this way yet, however, and so far I have not felt the need, as it seems fairly easy to achieve a glow discharge by other means.

I would like, at some point, to try semiconductor preionization, which has worked well for me in reduced-pressure nitrogen lasers. To do this, I would put a stripe of epoxy cement on the under surface of the glass “roof” of the channel; while the epoxy is freshly mixed and newly applied, I would sprinkle fine-grind (FFF) silicon carbide grit into it. There needs to be a 1-mm-wide gap down the middle, but there are many ways to provide that. Once the epoxy has set and I have shaken off the excess grit, I will use electrically conductive paint to coat the region just outside the epoxy and onto the edge of it, so that the electrodes can supply voltage to the preionizer. (Diagram to follow, if and when I actually get around to trying this method.)

The next issue is the upper capacitor plates. I purchased a 6-inch-wide brass kickplate at the hardware store, and sawed two 8" pieces from it for my initial design. The kickplate was stamped or sheared from a larger piece of brass, so the edges were reasonably straight and smooth. It was slightly curved, so I had to flatten the pieces a little, but a few short sessions of flexing them by hand and observing the results got them flat enough to be usable.

It also helps to have a power supply. I bought an inexpensive Wimshurst machine, as I did not really have time to build one; but I hope to construct either a Voss (Toepler-Holtz) machine, or what amounts to a horizontal Carré machine at some point. Here is the Wimshurst in operation, clearly showing that it can produce more than enough voltage for my needs:

I did make some modifications; the original brushes were wires cut from pieces of window screen, and they were tearing up the sectors, which are just aluminum paint, apparently sprayed onto the disks through a mask. (If you are building your own generator, btw, you should be aware that Jarrod and others have discovered that India ink works quite well.) I pulled out the stiff wire and substituted Litz wire, which is fine and soft. It has problems, too, but at least it isn’t destroying the machine. At Jarrod’s suggestion, I also put a wooden ball on the end of each collector. I had not done this when I took the photo, so you can see (dimly, through the transparent plastic bar and the rotating disks) the original sharp-cut ends of the collectors, which are lossy.

To assemble the laser, I took a flat brushed-steel tray with raised sides, and put a piece of drawer liner in it. Initially, I did not even bother to remove the thin blue plastic protective sheets that were on both faces of the liner. Then I put the capacitor plates down on top of the liner, and added two lugnut covers as a spark gap, as Jarrod does, except that I put conductive paint between each lugnut cover and the metal it sits on, to improve the connection and reduce sparking.

Here is the base of the laser, with the drawer liner and the capacitor plates (and a cuvette of Fluorescein) in place:

Note the resistor string, and the positions of the lugnuts. (The piece of copper shim stock with the white cliplead on it is for attaching the EG&G GP-70 spark gap I mentioned above.)

I tried various items as electrodes, and eventually settled on one of the two drawer or door handles that you see at the left in the following picture, along with one of the 5/32" brass rods at the right.

I bought the drawer pulls at the hardware store (they are solid stainless steel, about 1/2" thick and just over 8&5/8" long), and the brass rods at the local hobby shop. Bending the brass is easy if you have a propane torch; just be careful to grasp the end with a pair of pliers or Vise-Grips, and to avoid touching any hot metal with your hands.

I have carefully rounded and polished the ends of the steel bars, which were originally just beveled, to minimize the amount of fussing and sparking that will occur during the discharge.

(See below for an even simpler version.)



Adjustment and Operation

Note the separation between the lugnut covers, which is 8mm or so in the photo (that’s actually a fairly large separation; 6 or 7 mm is probably enough to begin with)), and the separation between the capacitor plates, which is somewhat less (but see below for specifics).

Fire the laser and note the location of the spark at or near the lugnuts. Chances are that it will be a “flashover” on the surface of the dielectric unless you have taken steps to prevent that, as I did on my next laser (see photos, below). If you only see a few of these (say, half a dozen or so) before the spark gap begins to operate, that’s probably okay; if, on the other hand, you see lots of them, and the spark gap just doesn’t seem to want to work, you have a few choices:

  1. You can decrease the distance between the lugnuts by moving the capacitor plates. This decreases the firing voltage of the spark gap. It also decreases the amount of drive on the laser channel, and in the worst case it is possible to get a nice clean discharge without any indication of lasing.

  2. You can use a larger sheet of plastic, provided that there is room for it on your base. It is best to overlap the edges of the baseplate, something I couldn’t do on this laser because the base has walls at its edges. While overlapping the base is extremely helpful, it doesn’t deal with the region directly under the lugnut covers. (See next item.)

  3. You can put obstructions on the dielectric, between the lugnut covers (or whatever you are using as spark gap electrodes), to make the surface path longer and thus discourage sparks. I did this on the next laser, and it worked quite well. (See photos, below.)

When you have the spark gap firing cleanly, observe what happens between the electrodes. What you want to see is a lot of small white sparks, distributed across essentially the entire length of the channel:

(There is a resistor blocking your view of the dye cuvette, but I can assure you that the laser is not lasing in this photo.)

If you see a lot more sparks at one end than at the other, you get to short out the electrostatic generator so you don’t get a rude surprise, and then carefully reorient the capacitor plates so the edges are closer to parallel. (You will find that they are difficult to move, because charging them up puts rather strong forces on the capacitor, and that squeezes a lot of the air out. Take your time, and be gentle.) It is best to use a shim of uniform thickness between the plates, to be sure that the facing edges (which should be straight) are parallel to each other. I have various pieces of wood and plastic that I use for this purpose.

Notice, though, that there are hardly any sparks in about the last 3/8" of the channel at the end nearest the camera in the photo; a difference that small is probably ignorable.

[I see a lot of photos of TEA nitrogen lasers with huge weights holding the capacitor plates down to the surface of the dielectric. If your base is reasonably flat and your capacitor plates are reasonably flat, that is completely unnecessary. The electric field will provide plenty of force. OTOH, it is important to make sure that the connection between each capacitor plate and its channel electrode is good, and weights can be very helpful there.]

Once you have good sparking all the way along the channel, you can put your electrodes on the laser and begin to position them. (You can look down on the brass rod from above and wiggle it a bit until just the edge of the capacitor plate is visible under it, all the way across. Then you can edge it just a little further out into the gap, carefully keeping it parallel to the edge of the plate. This takes some practice, so give it time and keep playing with it until you get it right. Also, see this page for a reasonably easy way to make small adjustments.)

Here is what the laser looks like with the smaller rod in place as its anode, and the larger one as its cathode:

Note the fact that the leading edge of each of the electrodes is slightly beyond the edge of the capacitor plate that it sits on. Both Jarrod and I are still looking into this; there is at least one suggestion in the literature (in an article by Ernest E. Bergmann in Applied Physics Letters, V28N2, 15 January, 1976) that allowing the edge of one capacitor plate to protrude slightly can improve preionization, and we need to try that to see whether we get similar results.

The rods are not likely to be positioned correctly at this point, and when you fire up the laser you will probably see something that resembles this, though of course it won’t be identical:

The purplish glow at the far end is what you want to see in the entire channel. If you look carefully at the sparks, you will notice that they are jumping between the capacitor plates, not between the electrodes; this is a clear sign that the electrodes are too far apart where the sparks occur (in this case, at the end closer to the camera), so I gently tapped the near end of the steel rod to bring it a fraction of a millimeter closer to the brass rod. Here is the result:

(Thanks to Milan Karakas for tweaking this photo to make it much easier to see what’s going on.)

The large stainless-steel rod is not a particularly good electrode for this type of laser; it is very easy to get a clean discharge with large rods, but harder to get the laser to reach threshold. Moreover, air is a terrible lasing medium, and this laser is far from optimized, so it just barely reached threshold.

You can see a reasonably even purple glow in the channel. That’s the desired condition. (There are, however, two bright spots on the left side, which are not desired.) Please remember that the flat brass bar that you see on the left side of the channel is just a weight; the actual anode is the round brass rod underneath it. You can tell this by the fluorescence on the dye cuvette, which is a slanted line. (Look to the left of the white pill-bottle, below and to the left of the resistor.)

(To get a better view, click the small image and then change “12c” in the filename to “22c”. The larger image is my attempt to perform the same enhancement that Milan performed on the smaller one; I confess that I was less successful.)

Note that if sparks jump between the electrodes, this can be a sign that they are too close together. It can, alternatively, be a sign that the something else is out of adjustment; I will mention one specific possibility in my description of the next version of this laser.

I tend to use rods of slightly different sizes as my electrodes, btw, with the cathode being a bit smaller than the anode; but Jarrod reports that he gets his best results when he uses rods that are the same diameter.

(10 April, 2007)

Last night, I tried several things. The first was to put a commercial power supply on the laser. This allowed me to get a sense of the operating voltage. With a spark gap spacing of 8 mm or so, I had to apply about 22.4 kV to the laser to get it to fire. Because the gap is free-running, this value varies from shot to shot, and I am not 100% certain of the calibration of my variable transformer or my power supply, so let’s just call it 22.5 kV. (At about 7 mm spacing, the value decreases to about 20.5 kV.)

I found that I could get some lasing with air, and that when I put nitrogen in the channel the spot on the cuvette got a lot brighter. This is expectable.

Then I removed the thin blue protective sheets from the drawer liner plastic, set the spark gap spacing at about 7 mm, and tried again. The results were very similar. The increased capacitance of the slightly thinner dielectric appears to compensate for the slightly lower voltage.

At that point I put the GP-70 triggered spark gap on the laser, reduced the voltage to 20 kV (the maximum rated voltage for the GP-70), and found that although I could not get a really clean discharge (there were always at least a few white sparks), and was unable to obtain lasing with just air in the channel, I seemed to be getting better performance with nitrogen with the triggered spark gap than with the free-running gap.

I will, however, have to retest to be sure; other parameters almost certainly changed, which means that this result does not constitute a proper test. (For one thing, the electrode spacing and possibly also the capacitor plate spacing spacing were different, because I had to move things around in order to change gaps.)



More About Alignment; Another Version of the Laser

(03-04 May, 2007)

Because I want to make some measurements, I threw together another version of the laser. This one has a base without any walls, and the dielectric overlaps it almost everywhere. This turns out to be a big help in avoiding flashovers from the edges and corners of the capacitor plates, and I have decided that it is an important design point.

In order to avoid flashovers under the spark gap, which is the one place where I had to chop a hole in the dielectric, and where there would be a path in any case, I put two little ABS or styrene plastic “H” beams (turned on their sides, so they are really being “I” beams) on the dielectric. The I-beams are held in place with “corona dope”, high-voltage insulating varnish. Here’s a photo from May 3rd:

(The piece of PVC tube blocks the light from the spark gap, which would otherwise cause very bright fluorescence in the dye, and make it hard to see the laser’s output.)

The capacitor plates of this laser are 6"x10", and I am using electrodes that are 12" long. I have not yet tried adding a rear mirror to this laser, but because the total pulsewidth is not much more than 1 nsec, and light travels about 1 foot in 1 nsec, a rear mirror probably won’t do much good. The only way to be sure, however, is to try it.

The anode is a brass rod, 3/16" in diameter, and the cathode is a flat brass bar that is 3/32" thick and 1/4" or 5/16" wide. I have rounded and smoothed the ends of both of these, but did not do any other special preparation. (I am taking advantage of the fact that the bar seems to have been sliced from a sheet of brass, and has slightly sharp edges.) The electrodes are held down on the capacitor plates by modest weights, as you can see in the photos.

I used essentially the same alignment procedure as before: I put the electrodes in place, fired the laser, and noticed that because of their shapes and the fact that the edge of the bar was just about vertically above the edge of the capacitor plate the spacing was very wide, so I got lots of long white sparks. I took the electrodes off, moved the plates a little closer together (they are now perhaps 5mm apart), put the electrodes back on, and fired the laser again.

There were a few white sparks, but the laser lased anyway.

I then moved the bar a little closer to the rod, and got this:

My apologies for the small size of the image; it’s a crop, and the camera lens was not set to full telephoto. Here is a larger one, from May 4th:

(If you want slightly more detail, click the small image and then change the filename of the large one to c0438c.flatround.airlase.c17.jpg — that will give you the original crop.)

You can see what Jarrod Kinsey refers to as “icicle sparks” on the cathode side of the channel, which is on the right in the first photo and on the left in the second; and you can see a fairly bright spot on the cuvette, which in the first case is filled with Rhodamine 6G in isopropanol, and in the second is filled with 7-Diethylamino-4-Methyl-Coumarin, also in isopropanol. (In both photos, the cuvette is out of focus.)

I have, btw, cleaned up some bad pixels so they don’t distract; but the photos have not been messed with otherwise, except to scale them.

Here is an end view, taken on May 3rd, showing the working alignment:

The flat protrudes further past the edge of the capacitor plate than the rod does. I will note that I have observed an increased tendency to spark when the anode (rod) is not far enough out; if you find that you cannot eliminate white sparks or get a clean discharge by moving the electrodes closer to and farther from each other, check the position of the rod above the edge of its capacitor plate. Also, check to see that the edges of the plates are parallel to each other, and that the electrodes are parallel to the plates.

As of May 4th, I started using slightly larger weights (3/4" bolts, 6" long, in pairs) to hold the electrodes in firm contact with the capacitor plates, and as of May 6th I am using a stack of three such bolts on top of a glass “roof”:

Here is a view into the end of the channel. My apologies for the poor focus.

Relatively modest voltage (the spark gap spacing is only 5 mm) is enough to pump 7-Diethylamino-4-Methyl-Coumarin, if the laser channel is filled with nitrogen. Here is a photo showing the gap spacing:

The blue dye-laser output spot on a paper target is somewhat diffuse, as one would expect when the dye is driven to superfluorescence by a relatively short and wide pump geometry. Here is a photo, taken on May 6th; the spark gap spacing was increased to 8 mm, there was nitrogen in the channel, and a cylindrical lens focused the nitrogen laser’s output onto the dye cuvette:

The output (which is on a tilted paper target, in case you were wondering about the slant) is left of center, and the dye cuvette is near the right edge of the image. You can see a bright spot in the middle of the output; my best guess is that this is the result of reflections off at least one of the walls of the cuvette, and the more diffuse blue line above and below it is probably superfluorescent lasing. (The blue dot slightly to the right of the vertical line is less easy to understand, but may be the result of a multiple bounce off slightly misaligned surfaces.)

The combination of a flat cathode with a somewhat sharp edge and a [slightly larger] round anode appears to be a good one. Also, it is clear that if the electrodes are long enough to extend about an inch beyond the capacitor plates at each end, they do not need to have particularly special shapes. (I used a file to round the ends, and 600-grit sandpaper to smooth them; I did not make any attempt to polish them.)

(10 May, 2007)

I tried a quarter-inch steel rod instead of the flat, and got good enough performance that I was able to lase 7-Diethylamino-4-Methyl-Coumarin with just air in the channel. This photo was taken from behind the cuvette:

It is quite difficult to lase dye with an air laser; you’ll notice that the dye laser’s output spot on the target at left is small and not extremely bright.

Here is an overview of the laser, with the weights removed so you can see the rods:




Operating Parameters and Related Considerations

To achieve 100 Volts per Torr centimeter, which is approximately the optimum for nitrogen laser operation, we need to put just under 23 kV across the channel if the electrodes are 3 mm apart. The impedance of the channel is changing constantly during the discharge cycle, and is not really ohmic, but we can think of it as starting at infinity and decreasing rapidly to a value that is, at least in typical “TERP” lasers, at most a few tenths of an ohm.

An LC-inversion circuit puts nearly twice its initial charging voltage across an open circuit, so if I start with a charging voltage of 20 kV I should have no trouble exceeding 23 kV.

(The optimum seems to be fairly broad or ill-defined, with some researchers reporting values closer to 80 V/T*cm and others reporting values as high as 200 or so. I chose 100 because it is a convenient number.)

As I report above, I got very decent lasing with a channel spacing on the order of 3 or 4 mm and initial charge voltage of ~20 kV. Whether it is well optimized, however, is another story. Fairly extensive further testing will be required before I can really answer that question.



Links

To a set of references to significant articles about nitrogen lasers

To the first page in this set, a general discussion of the issues involved in designing and building a high-performance nitrogen laser

To Jarrod Kinsey’s pages

To Milan Karakas’s pages

To a page about a high-performance nitrogen laser that is a charge-transfer circuit rather than an LC-inversion circuit, and uses water as the dielectric in its peaker capacitor

Back to the Index

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This work is supported by
the Joss Research Institute
19 Main Street
Laurel MD 20707-4303 USA



Contact Information:

My email address is a@b.com, where a is my first name (just jon, only 3 letters, no “h”), and b is joss.

My phone number is +1 240 604 4495.

Last modified: Fri Jun 8 16:22:20 EDT 2007